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010 _a 2022058434
020 _a9780367775018
020 _a9781032013220
020 _z9781003178187
040 _aLBSOR
_beng
_erda
_cLBSOR
041 _aeng
042 _apcc
049 _aBEV
050 0 0 _aQD850
_b.M433 2023
082 0 0 _a541/.39
_223/eng20230511
092 _223
_a541.39
245 0 0 _aMechanochemistry and emerging technologies for sustainable chemical manufacturing /
_cedited by Evelina Colacino, Felipe Garcia.
264 1 _aBoca Raton, Florida :
_bCRC Press,
_c2024.
300 _a316 pages :
_billustrations; graphics;
336 _atext
_btxt
_2rdacontent
337 _aunmediated
_bn
_2rdamedia
338 _avolume
_bnc
_2rdacarrier
504 _aIncludes bibliographical references and index.
505 0 _aIntroduction : overview of book : objective of book : scaling up sustainable synthesis by mechanochemistry / Deborah Crawford, Felipe Garcia and Evelina Colacino -- Mechanochemistry : a brief historical introduction / Seplak Vladimir and Senna Mamoru -- In situ monitoring of mechanochemical reaction by Raman/PXRD / Ivan Halasz -- Kinetics and thermodynamics of mechanochemical reactions : a computational approach / Feliu Maseras -- The thermodymanics and kinetics of mechanochemical reactions : an experimental approach / Adam Michalchuk -- Life cycle assessment / Sabrina Spatari -- Intellectual properties in mechanochemistry / Tanja Benele -- Mechanochemistry at scale : the ultimate process intensification and beyond including continuous mechanochemical synthesis by twin screw extrusion Identification of important parameters moving forward / Valerio Isoni -- Batch mechanochemical synthesis : scale-up / Michael Fellderhoff -- Acoustic synthesis (solvent-free) and resonant acoustic mixing (RAM) / Maria Rivas-Velazco -- Case study : sustainable large scale manufacturing of fine chemicals, APIs and biologically active compounds / Bela Torok -- Case study : Siebtechnik Company (DE) and eccentric mills / Peter Balaz -- Scalable solutions for continuous manufacturing by mechanochemical-assisted synthesis / Duncan Browne -- Large scale continuous flow chemistry / Darren Riley -- Sustainable chemical manufacture in water : An industrial point of view / Fabrice Gallou.
520 _a"This unique volume describes advances in the field of mechanochemistry, in particular the scaling up of mechanochemical processes. Scalable techniques employed to carry out solvent-free synthesis are evaluated. Comparability to continuous flow chemistry, the current industrial benchmark for continuous efficient chemical synthesis, is presented. The book concludes that mechanochemical synthesis can be scaled up into a continuous, sustainable process. It demonstrates that large scale mechanochemistry can meet industrial demands especially in the pharmaceutical industry. The case studies conducted on MOF Technologies and Deasyl demonstrate how mechanochemistry is employed on a pilot plant scale"--
650 0 _aMechanical chemistry.
650 0 _aChemical processes
_xTechnological innovations.
700 1 _aColacino, Evelina,
_eeditor.
700 1 _aGarcĂ­a, Felipe
_c(Chemist),
_eeditor.
906 _a7
_bcbc
_corignew
_d1
_eecip
_f20
_gy-gencatlg
942 _c6
_2ddc
_e23
_h541
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