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Chromatography has become the most widely used technique for separation and analyses. Because a great deal of information is available on the three main types--gas chromatography (GC), liquid chromatography (LC), and thin layer chromatography (TLC)--they are usually treated separately despite their common theoretical base. This comprehensive work presents a unified study of chromatography which introduces the principles shared by each method while emphasizing the similarities and differences between the three types. The chapters covering these methods build on the introductory coverage of common principles, providing an effective overview of the subject for novices and allowing practitioners to more easily switch from one technique to another. In addition, this approach permits the use of one set of terms and symbols, making learning easier. Includes several practical examples the ways in which GC, LC, and TLC operate, as well as a section on special techniques such as chiral separations and derivatization.

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• Preface to Second Edition
• Acknowledgments
• Preface to the First Edition
• Symbols, Abbreviations, and Acronyms
• 1 Impact of Industrial and Government Regulatory Practices on Analytical Chromatography
• 1.1 Locus of Chromatography in Chemical Industry
• 1.2 Governmental Organizations
• 1.3 Nongovernmental Agencies
• 1.4 Standards, Calibration, and NIST
• 1.5 USP and Other Pharmacopoeias
• 1.6 International Guidelines for Analytical Laboratories
• 1.7 Final Comments
• References
• 2 Introduction to Chromatography
• 2.1 Brief History
• 2.2 Definitions and Classifications
• 2.3 Summary
• References
• 3 Band Broadening and Kinetics
• 3.1 Configurations of the Stationary Phase
• 3.2 Rate Theory
• References
• 4 Physical Forces and Interactions
• 4.1 Intermolecular and Interionic Forces
• 4.2 Size Exclusion-Molecular Sieving
• 4.3 Some Models
• References
• 5 Optimization and the Achievement of Separation
• 5.1 Kinetics and Zone Broadening
• 5.2 Thermodynamics and Zone Migration
• 5.2 Achievement of Separation
• 5.4 Optimization of Separations
• References
• 6 Comparisons Between Chromatographic Modes
• 6.1 Gas Chromatography Compared to Liquid Chromatography
• 6.2 Supercritical Fluids and Supercritical Fluid Chromatography
• 6.3 Reduced Parameters
• 6.4 Columnar and Planar Configurations
• References
• 7 Gas Chromatography
• 7.1 Early History, Theories, and Classifications
• 7.2 Instrumentation for Capillary GC
• 7.3 Instrumentation for Packed-Column GC
• 7.4 Stationary Phase
• 7.5 Temperature Effects
• 7.6 Special Topics
• 7.7 Summary and Evaluation
• References
• 8 Liquid Chromatography in Columns
• 8.1 Introductory Classifications
• 8.2 Classification of HPLC Modes
• 8.3 Instrumentation
• 8.4 Reversed-Phase Method Development and Optimization
• 8.5 RP-HPLC Alternatives for the Pharmaceutical Industry
• 8.6 Preparative LC
• 8.7 Special Topics
• 8.8 Summary and Evaluation
• References
• 9 Quantitation: Detectors and Methods
• 9.1 Detectors
• 9.2 Data Acquisition and Processing
• 9.3 Quantitative Analysis
• References
• 10 Chromatography with Mass Spectral Detection (GC/MS and LC/MS)
• 10.1 Basics of Mass Spectrometry
• 10.2 Gas ChromatographyrMass Spectrometry
• 10.3 Liquid ChromatographyrMass Spectrometry
• 10.4 Other Hyphenated Methods
• 10.5 Summary
• References
• 11 Liquid Chromatography on Plane Surfaces
• 11.1 Paper Chromatography
• 11.2 Thin-Layer Chromatography
• 11.3 Other Topics
• 11.4 Literature Summary and Applications
• References
• 12 Qualitative Analysis
• 12.1 Retention Parameters
• 12.2 Other Methods of Qualitative Analysis
• References
• 13 Capillary Electrophoresis and Capillary Electrochromatography 365
• 13.1 Principles of Electrophoresis
• 13.2 Zone Electrophoresis
• 13.3 Capillary Electrophoresis
• 13.4 Capillary Electrochromatography
• References
• 14 Sample Preparation
• 14.1 Extraction
• 14.2 Dialysis
• 14.3 Derivatization
• References
• 15 Special Applications
• 15.1 Multidimensional Chromatography
• 15.2 Biological Applications
• 15.3 Chiral Separations
• 15.4 Other Topics
• References
• 16 Selection of a Method
• 16.1 Methods of Attack
• 16.2 The Internet
• 16.3 Experimental Approach
• 16.4 Summary
• References
• Some Internet Web Sites of Interest to Chromatographers
• Appendix A ICH Glossary
• Appendix B Index

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CHOICE Review

This new edition of Miller's book (1st ed., CH, Sep'88, 26-0317) is a 15-year expanded update of the original work. The additional material covers newer chromatographic techniques and applications, sample preparation, expanded theoretical material, current industrial and government rules/procedures, and Internet resources. Miller (emer., Drew Univ.) begins with an extensive section on chromatographic symbols, abbreviations, and acronyms. The content is adequately referenced at the end of the chapters, and the numerous illustrations are valuable adjuncts to the material presented. Even though this book is referred to as a textbook, no problem sets are included. The book is written from a practical, hands-on approach and the reader is constantly sent to other works for extended detail on a topic or technique. ^BSumming Up: Recommended. Upper-division undergraduates through professionals/scientists employing chromatographic analyses. J. F. Belliveau Providence College