03506cam a22004098i 4500 23025577 OSt 20250220152142.0 230318s2023 flu b 000 0 eng 2022058434 9780367775018 9781032013220 9781003178187 LBSOR eng rda LBSOR eng pcc BEV QD850 .M433 2023 541/.39 23/eng20230511 23 541.39 Mechanochemistry and emerging technologies for sustainable chemical manufacturing / edited by Evelina Colacino, Felipe Garcia. Boca Raton, Florida : CRC Press, 2024. 316 pages : illustrations; graphics; text txt rdacontent unmediated n rdamedia volume nc rdacarrier Includes bibliographical references and index. Introduction : overview of book : objective of book : scaling up sustainable synthesis by mechanochemistry / Deborah Crawford, Felipe Garcia and Evelina Colacino -- Mechanochemistry : a brief historical introduction / Seplak Vladimir and Senna Mamoru -- In situ monitoring of mechanochemical reaction by Raman/PXRD / Ivan Halasz -- Kinetics and thermodynamics of mechanochemical reactions : a computational approach / Feliu Maseras -- The thermodymanics and kinetics of mechanochemical reactions : an experimental approach / Adam Michalchuk -- Life cycle assessment / Sabrina Spatari -- Intellectual properties in mechanochemistry / Tanja Benele -- Mechanochemistry at scale : the ultimate process intensification and beyond including continuous mechanochemical synthesis by twin screw extrusion Identification of important parameters moving forward / Valerio Isoni -- Batch mechanochemical synthesis : scale-up / Michael Fellderhoff -- Acoustic synthesis (solvent-free) and resonant acoustic mixing (RAM) / Maria Rivas-Velazco -- Case study : sustainable large scale manufacturing of fine chemicals, APIs and biologically active compounds / Bela Torok -- Case study : Siebtechnik Company (DE) and eccentric mills / Peter Balaz -- Scalable solutions for continuous manufacturing by mechanochemical-assisted synthesis / Duncan Browne -- Large scale continuous flow chemistry / Darren Riley -- Sustainable chemical manufacture in water : An industrial point of view / Fabrice Gallou. "This unique volume describes advances in the field of mechanochemistry, in particular the scaling up of mechanochemical processes. Scalable techniques employed to carry out solvent-free synthesis are evaluated. Comparability to continuous flow chemistry, the current industrial benchmark for continuous efficient chemical synthesis, is presented. The book concludes that mechanochemical synthesis can be scaled up into a continuous, sustainable process. It demonstrates that large scale mechanochemistry can meet industrial demands especially in the pharmaceutical industry. The case studies conducted on MOF Technologies and Deasyl demonstrate how mechanochemistry is employed on a pilot plant scale"-- Mechanical chemistry. Chemical processes Technological innovations. Colacino, Evelina, editor. García, Felipe (Chemist), editor. 7 cbc orignew 1 ecip 20 y-gencatlg 6 ddc 23 541 303548 303548 0 0 ddc 0 0 10 10 1 2025-02-20 19 51.93 1 541.39 M4649 2024 80000002670340 2025-04-14 09:23:28 2025-02-26 51.93 2025-02-20 6