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Descripciones mejoradas de Syndetics:
Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
"A Wiley-Interscience publication."
Includes bibliographical references and index.
Tabla de contenidos provista por Syndetics
- Preliminary Stages?
- X-Rays?
- Diffraction of X-Rays?
- Crystals, Symmetry, and Space Groups?
- Crystals and Their Properties?
- Geometric Data Collection?
- Intensity Data Collection?
- Data Reduction?
- Theory of Structure Factors and Fourier Syntheses?
- Calculation of Structure Factors and Fourier Syntheses?
- The Phase Problem?
- The Phase Problem?
- Direct Methods?
- Patterson Methods?
- Heavy Atom Methods?
- Search Methods?
- Completing the Structure?
- Refinement and Results?
- Refinement of Crystal Structures?
- Random and Systematic Errors?
- Derived Results?
- Ambiguities and Uncertainties?
- Appendices?
- Index
Notas de autor provistas por Syndetics
George H. Stout and Lyle H. Jensen are the authors of X-Ray Structure Determination: A Practical Guide, 2nd Edition, published by Wiley.